FreeZone Triad Benchtop Freeze Dryers are designed for multiple types of lyophilization: flask, bulk and stoppering vials. With the ability to freeze dry samples in so many different forms, the Triad’s versatility and compact design make it perfect for busy labs.
The upright stainless steel collector coil holds 2.5 liters of ice before defrosting. Two 1/3 hp HCFC/CFC-free refrigeration compressors cool the collector to -85° C (-121° F), suitable for aqueous or dilute acetonitrile samples. Temperature-controlled shelves range from -55° C to +50° C (-67° F to +122° F) and a maximum of -75° C (-103° F) during pre-freezing. The shelves provide pneumatic stoppering with a diaphragm, eliminating the need for compressed gas.
Lyo-Works™ OS provides a real time display of collector temperature and vacuum level, shown on a 5″ full color, capacitive touchscreen. A stoppering tray dryer and four valve ports are built-in.
Vacuum pump and freeze dry glassware (if not bulk freeze drying) are required (not included).
Features (All Models)
Stainless steel collector coil capable of removing 1.84 L of water in 24 hours and holding 2.5 L of ice before defrosting
Two 1/3 hp HCFC/CFC-free refrigeration compressors cool the collector to -85° C (-121° F) and work in concert with a 1000-watt heater to cool and heat fluid medium circulating through channels in the shelf. Not for use with samples containing methanol or ethanol
Processing shelf, 12.4″ w x 14.5″ d (31.5 x 36.8 cm). Spacing between shelf and top of chamber accommodates containers with stoppers up to 148 mm maximum height
One probe for monitoring temperature of sample in chamber
Temperature ramp and hold programming from -55° C to +50° C (-67° F to +122° F) and -75° C (-103° F) during pre-freezing. Controls temperature to ±1° C of set point. Memory to store 30 programs with 16 segments each including number of steps, ramp rate, shelf temperature, hold time and vacuum level
Full color, 5″ capacitive touchscreen with Lyo-Works™ OS:
Real time display of collector temperature and vacuum level
Creation and storage for up to 30 programs with up to 16 steps each. Ability to set ramp rate, shelf temperature, shelf temperature time and vacuum set point per step
Manual start-up buttons for collector and shelf temperature control and vacuum pull down
Alerts, diagnostic tests, user manual and defrost control
Data logging stores and displays data in table or graph format, and may be exported via USB or Ethernet
Settings include language (English, Spanish, French, German, or Italian), time, temperature (° C or ° F) and vacuum (mBar, Torr or Pa)
Alerts can be emailed to user-entered addresses via Ethernet connection
Vacuum pump maintenance alert
Security lock-out
Pneumatic stoppering mechanism with diaphragm and plate. No compressed gas is required
Stoppering control knob, vacuum release control knob and 1/8″ OD user-supplied sterile/inert gas backfill port
Four left side-mounted neoprene valves with molded plastic knobs and fittings that accommodate 1/2″ and 3/4″ flask adapters
USB port and Ethernet connection
Electrical receptacle for vacuum pump
Hot gas defrost with stainless steel drain pan, silicone drain hose and auto shut off at +60° C (+140° F)
Vacuum control valve
Vacuum break valve
Stainless steel and powder-coated steel exterior
Clear acrylic door, 1″ thick, with silicon gasket and latch 3/4″ OD vacuum connection. 36″ long, 3/4″ ID vacuum hose with two clamps
Options Include
Region-specific electrical plug configurations
Required Accessories (Not Included)
Vacuum pump with a displacement of at least 98 L/min, 0.002 mBar ultimate pressure and fitting for 3/4″ ID vacuum hose
Freeze dry glassware if not bulk freeze drying